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AICl 3 is the most frequently used catalyst in aromatic Friedel-Crafts acylations, but other Lewis acid metal halides also show high activity and are applied accordingly. Considering relative efficiencies of metallic halides (most of which were discussed in reference to Friedel-Crafts alkylations), these are also relevant for FriedelCrafts acylations (see Section 5.1.4). In short, since the activity of Lewis acid metal halides depends on the reagents and reaction conditions, relative reactivity orders may be established for a given reagent only under given reaction conditions. On the basis of their activity in the acetylation with acetyl chloride of toluene, SbCI s, FeCI 3, SnCI 4 , and TiCl 4 are also efficient catalysts, whereas ZnCl 2 is usually a relatively weak Lewis acid in Friedel-Crafts acylations ,4 It is interesting to note that in the solvent-free aroylation of benzene and toluene under microwave irradiation with various Lewis acid chlorides, including AICI 3, FeCl 3 exhibited by far the best activity. 39 Boron trifluoride complexes are also often applied. BF3 when used with acyl fluorides showed in some cases distinct differences compared to other catalystreagent combinations. For example, acylation of 2-methylnaphthalene with isoBuCOF and BF3 gives high yield (83%) of the 6-substituted isomer in contrast to AICl 3 (30%).40 A similar example is shown here:

For example, charset="ISO 8859-1" For example, hreflang="en-US" alternate stylesheet start next prev contents index glossary copyright chapter section subsection appendix help bookmark alternate stylesheet start next prev contents index glossary copyright chapter section subsection appendix help bookmark Any valid MIME type

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5 . One of the first ion thrusters to fly in space was a cesium surface ionization thruster where cesium ions were pulled from a hot surface by the electric field that also produced the beam. Model the thruster as a diode, with cesium ions at 7.5 d c m 2 coming from one surface and with the other electrode an accel grid with 80% transparency and a grid gap d from the ion source. a. Assuming 100% mass utilization efficiency, neglecting the angular divergence of the beam, and using a 200-V negative bias on the accel grid, what is the voltage, current, thruster diameter, and gap size required to produce 5 mN of thrust at an Isp of 3000 s b. If the thruster has 95% mass utilization efficiency and a total angular divergence of the beam of 10 deg, how does that change the results of part (a) c. If it takes 100 W of power to heating the cesium ion-emitting surface to the required surface temperature of about 1350 K, what is the total efficiency of the thruster, using the parameters from part (b)

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Bilinear This method determines the values of new pixels by calculating a weighted average of the 4 closest pixels (a 2 2 array) based on distance. The quality is not as good as Bicubic but the process takes less time. Nearest Neighbor This method does not use an algorithm; instead, new pixels are created by using the values of the nearest neighbor. It s used mainly on images that contain hard edges, such as illustrations and screenshots. When an image is enlarged using this method, it can appear noticeably jagged. When an image is reduced in size, it can appear noticeably grainy.

Figure 11.6 Worldwide Condor ock ca. 1994. This is a map of the worldwide Condor ock in 1994. Each dot indicates a complete Condor pool. Numbers indicate the size of each Condor pool. Lines indicate ocking via gateways. Arrows indicate the direction that jobs may ow.

However, instead of trying to derive explicit expressions for [E], [ES] and [EP] and then substituting these back into Equation (8.49), the King Altman approach seeks rst to construct a vector equivalent diagram linking all the biocatalyst species together (Figure 8.34). Expressions for [E], [ES] and [EP] are then derived by considering all the alternative pathways to any given species starting from one or other or both of the other biocatalyst species (Figure 8.34). The result is [E] k 2 k 1 + k 1 k3 + k2 k3 [ES] k 2 k1 [S] + k3 k1 [S] + k 3 [P]k 2 [EP] k1 [S]k2 + k 1 k 3 [P] + k2 k 3 [P] (8.50) (8.51) (8.52)

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